Beamline Phone Number:
+44 (0) 1235 778889
Principal Beamline Scientist:
Giuliano Siligardi
Tel: +44 (0) 1235 778425
E-mail: giuliano.siligardi@diamond.ac.uk
Email: robert.rambo@diamond.ac.uk
Tel: +44 (0)1235 56 7675
Parameter |
Availability |
Comment |
Spectral range
|
Module B |
190-650nm |
Module A |
125 - 500nm |
|
Beam size at sample
|
available |
0.5mm2 to 2mm x 4mm |
Flux at sample
|
available |
0.9 × 1012 (Module A) 3.2× 1012 (Module B) (ph/s/0.1% bw at 200nm), 300mA |
Equipment or Component |
Availability |
Comments |
Customised UHV Olis DSM20 monochromator
|
available |
under ultra high vacuum (UHV) scanning 125-500nm |
Detector
|
available |
Photo multiplier tube with MgF2 window |
Sample compartment
|
available |
For standard cylindrical, rectangular and demountable cells. N2 Purged compartment |
Linkam System | ||
6-cell turret for rectangular cells (0.1 mm, 0.2 mm, 0.5 mm, 10mm pathelength cells) | ||
HT-CD (multiplate or multicell system) | ||
MCD (rectangular cuvette of 0.02, 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 1cm in pathlength) | ||
Temperature Controller |
|
Linkam System -150-350° C |
Quantum Peltier 5-90° C |
Equipment or Component |
Availability |
Comments |
|||||
Mueller Matrix Polarimeter |
Available |
under N2 scanning 190-650nm |
|||||
Detector
|
available |
Photo multiplier tube |
|||||
Measurement mode
|
available |
Circular Dichroism Linear Dichroism Absorbance Circular Birefringence Linear Birefringence |
Mapping | ||||
Spectra | |||||||
Temperature controller | available | Linkam -170 to 300° C | |||||
Acessories |
available |
1.3T magnetic field |
Pathlengths (cm) |
Availability |
Capacity (µl) |
Demountable cell (nominal pathlength: 2, 5, 10, 50, 100, 200 µm) Cylindrical & Rectangular cells 0.01 Cylindrical 0.02 Cylindrical 0.05 Cylindrical 0.1 Cylindrical & Rectangular 0.2 Rectangular 0.3 Rectangular 0.5 Cylindrical 1 Cylindrical & Rectangular 10 Rectangular
HT-CD cell strips: pathlength , 10 µm, 100 µm, 200 µm, 1cm |
available |
2-15µl
Full 200 µl (window 20 µl) Full 200 µl (window 30 µl) 150 µl 250 µl
50 µl - 450 µl 800 µl (small aperture)
10 µm (8 µl) 100 µm (12 µl) 200 µm (12 µl) 1cm (350 µl) |
Stereo Zoom Zeiss microscope | available | Reflection and Transmission mode 8x zoom for small objects Fiber optics illumination | ||
Nanophotometer | available | For UV-Vis absorbance 200-1100nm wavelength range | ||
pH meters | available | Smallest Ø=3mm probe | ||
Chemical fume cupboard | available | For nitric acid cell cleaning | ||
Concentrator | available | For Eppendorf vials | ||
Centrifuges | available | Minispin for Eppendorf vials Up to 15K rpm | ||
Fridge/freezer | available | Sparkfree Fridge 4°C Freezer -25°C | ||
Freezer -80°C | Available on demand | | ||
Analytical micro-balances | available | ± 1µg | ||
Water bath, hot plate heating, stirrers, ultrasound bath | available | |||
Thermomixer | available | For Eppendorf vials and standard rectangular cells |
For any further information, please contact a member of the beamline staff.
Diamond Light Source is the UK's national synchrotron science facility, located at the Harwell Science and Innovation Campus in Oxfordshire.
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OX11 0DE
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